... cylinders x 3 Stand x 1 Clamp x 1 Reagents Cyclohexanol, Saturated sodium chloride solution, anhydrous sodium sulphate, Bromine in chloroform, dilute alkaline potassium permanganate (VII) solution & Acetone. Procedure A. Apparatus set up 1. The still head was connected with a condenser. 2. This still head was connected with a screw cap with a 150? thermometer whose still head was located at the mouth of the condenser. 3. The junction between the still head and the condenser was wrapped up in a piece of aluminum foil. 4. This whole setup was clamped. 5. 2 rubber tubes were connected to condenser's water in (near the head) and the water out (near the tip). 6. Finally a clean & dry conical flask (put in the ice bath) was placed to near the tip of the condenser to collect the distillate. B. Preparation of the reagents 1. 15 cm3 of cyclohexanol was added in to a 50cm3 pear-shaped flask by using measuring cylinder. 2. 4.0cm3 ...

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